I-SepaFlash™ Standard Series Series
Amakholomu e-Standard Series flash anomshini opakishwe ngejeli ye-silica ye-UltraPure esebenzisa indlela yokupakisha eyomile yokuphathelene.
※ I-silica ye-UltraPure ihlanganisa ukusatshalaliswa kosayizi wezinhlayiyana eziqinile, izinga eliphansi lezinhlawulo kanye nokuqukethwe kwensimbi okune-trace ephansi, i-pH engathathi hlangothi, okuqukethwe kwamanzi okulawulwayo nendawo ephezulu, ihlinzeka ososayensi imiphumela yokuhlola efunwayo.
※ Inqubo yokupakisha eyomile eyingqayizivele, yokuphathelene iqinisekisa ukulungiswa okuphezulu kanye nokuphindaphindeka kokuhlanzwa kwansuku zonke.
※ Ingcindezi ethuthukisiwe ilinganiselwa ku-300 psi
| Inombolo Yento | Usayizi Wekholomu | Usayizi Wesampula(g) | Izinga lokugeleza(mL/min) | Ubude beCartridge (cm) | I-Cartridge ID (mm) | Ubukhulu. Ingcindezi(psi/bar) | Ubuningi/Ibhokisi | |
| Encane | Okukhulu | |||||||
| S-5101-0004 | 4 g | 4 mg–0.4 g | 15–40 | 105.8 | 12.4 | 300/20.7 | 36 | 120 |
| S-5101-0012 | 12 g | 12 mg–1.2 g | 30–60 | 124.5 | 21.2 | 300/20.7 | 24 | 108 |
| S-5101-0025 | 25 g | 25 mg–2.5 g | 30–60 | 172.7 | 21.3 | 300/20.7 | 20 | 80 |
| S-5101-0040 | 40 g | 40 mg–4.0 g | 40–70 | 176 | 26.7 | 300/20.7 | 15 | 60 |
| S-5101-0080 | 80 g | 80 mg–8.0 g | 50–100 | 248.5 | 30.9 | 200/13.8 | 10 | 20 |
| S-5101-0120 | 120 g | 120 mg–12 g | 60–150 | 261.5 | 37.2 | 200/13.8 | 8 | 16 |
| S-5101-0220 | 220 g | 220 mg–22 g | 80–220 | 215.9 | 59.4 | 150/10.3 | 4 | 8 |
| S-5101-0330 | 330 g | 330 mg–33 g | 80–220 | 280.3 | 59.8 | 150/10.3 | 3 | 6 |
| S-5101-0800 | 800 g | 800 mg-80 g | 100–300 | 382.9 | 78.2 | 100/6.9 | 3 | / |
| I-S-5101-1600 | 1600 g | 1.6 g–160 g | 200–500 | 432.4 | 103.8 | 100/6.9 | 2 | / |
| S-5101-3000 | 3000 g | 3.0 g–300 g | 200–500 | 509.5 | 127.5 | 100/6.9 | 1 | / |
※ Iyahambisana nazo zonke izinhlelo ze-flash chromatography emakethe.
| Inombolo Yento | Usayizi Wekholomu | Usayizi Wesampula(g) | Isilinganiso sokugeleza(mL/min) | Ubude beCartridge(cm) | I-ID ye-Cartridge(mm) | Ubukhulu. Ingcindezi(i-psi/ibha) | Ubuningi/Ibhokisi | |
| Encane | Okukhulu | |||||||
| I-S-8601-0004-N | 8 g | 8 mg–0.32 g | 10–30 | 105.8 | 12.4 | 300/20.7 | 36 | 120 |
| I-S-8601-0012-N | 24 g | 24 mg–1.0 g | 15–45 | 124.5 | 21.2 | 300/20.7 | 24 | 108 |
| I-S-8601-0025-N | 50 g | 50 mg–2.0 g | 15–45 | 172.7 | 21.3 | 300/20.7 | 20 | 80 |
| I-S-8601-0040-N | 80 g | 80 mg–3.2 g | 20–50 | 176 | 26.7 | 300/20.7 | 15 | 60 |
| I-S-8601-0080-N | 160 g | 160 mg–6.4 g | 30–70 | 248.5 | 30.9 | 200/13.8 | 10 | 20 |
| I-S-8601-0120-N | 240 g | 240 mg–9.6 g | 40–80 | 261.5 | 37.2 | 200/13.8 | 8 | 16 |
| I-S-8601-0220-N | awu 440g | 440 mg–17.6 g | 50–120 | 215.9 | 59.4 | 150/10.3 | 4 | 8 |
| I-S-8601-0330-N | awu 660g | 660 mg–26.4 g | 50–120 | 280.3 | 59.8 | 150/10.3 | 3 | 6 |
| I-S-8601-0800-N | 1600 g | 1.6 g–64 g | 100–200 | 382.9 | 78.2 | 100/6.9 | 3 | / |
| I-S-8601-1600-N | 3200 g | 3.2 g–128 g | 150-300 | 432.4 | 103.8 | 100/6.9 | 2 | / |
| I-S-8601-3000-N | 6000 g | 6.0 g–240 g | 150-300 | 509.5 | 127.5 | 100/6.9 | 1 | / |
※ Iyahambisana nazo zonke izinhlelo ze-flash chromatography emakethe.
Amakholomu e-flash e-SepaFlash™ anikeza ukusebenza okumangalisayo emikhiqizweni encintisanayo ngenxa yekhwalithi ephezulu yejeli ye-silica nezindlela zokupakisha ezintsha.
Le nto esebenza kahle kakhulu inesimo sezinhlayiyana esingajwayelekile esinamaphethelo abushelelezi, ukusabalalisa usayizi wezinhlayiyana ezincane kakhulu kanye nezinga eliphansi lezinhlawulo ezinikezwa u-Santai, okuzokwandisa amandla akho okuhlukanisa futhi konge isikhathi sakho nemali. Ijeli ye-silica engajwayelekile inezinhlobo ezimbili zokucaciswa, 40-63 µm kanye no-25-40 µm. Ikakhulukazi, u-Santai uyaqhubeka nokuthuthukisa indlela yokupakisha eyomile eqinile ye-silica engu-25-40 µm engajwayelekile, kanye nama-silica cartridges apakishwe ngaphambili angu-25-40 µm azobonisa ikhono elimangalisayo ekubhekaneni nokuhlukaniswa.
Isithombe se-SEM sejeli ye-silica engu-40-63 μm
Ijeli ye-silica ye-Santai iphinde inikeze lezi zinzuzo ngaphezu kwemikhiqizo esiqhudelana nayo:
I-pH emaphakathi:I-pH yejeli ye-silica ye-Santai igcinwa phakathi kuka-6.5−7.5. I-pH engathathi hlangothi iyadingeka ukuze kuhlukaniswe izinhlanganisela ezizwelayo ze-pH.
Okuqukethwe kwamanzi okuzinzile:Okuqukethwe kwamanzi kwejeli ye-silica kungathinta ukukhetha kwe-silica. Ijeli ye-silica ye-Santai engavamile inokuqukethwe kwamanzi okulawulwayo okungama-4% kuya ku-6%.
Indawo ephezulu:Indawo ephakeme (500 m2/g ye-60 Å usayizi wembotshana) inikeza amandla amakhulu okuhlukanisa.
Ukusatshalaliswa kosayizi wezinhlayiyana eziqinile kanye nokuphindaphindeka okuphezulu kwe-batch-to-batch: Ukusatshalaliswa kosayizi wezinhlayiyana ezincane kuzonikeza ukupakisha okufana kakhulu ukuze kuqoqwe izingxenyana ezigxilile futhi kunciphise ukusetshenziswa kwe-solvent, okuzonciphisa izindleko zizonke. Ukuphindaphindeka okuphezulu kwe-batch-to-batch kokusabalalisa usayizi wezinhlayiyana kuqinisekisa ngokuyisisekelo ukusebenza okuhle kakhulu kokuhlukana. Imininingwane eyengeziwe sicela ubheke isithombe se-SEM nokusabalalisa usayizi wezinhlayiyana zamaqoqo amabili.
Ukusabalalisa usayizi wezinhlayiya zamaqoqo amabili we-40-63 μm kanye ne-25-40 μm yejeli yesilika
Amakholomu e-SepaFlash™ aseyatholakala ngosayizi ongu-5 kg.
okungahlanza kufikela ku-500 amagremu wesampula ngesikhathi esisodwa.
I-spin-welded futhi ingamelana nengcindezi efika ku-100 psi (6.9 bar).
※ Ukusebenza okuthembekile, okungaguquki kusuka kuhlelo lokupakisha lobunikazi.
※ Umzimba we-cartridge oqinisiwe onengcindezi yokusebenza ephezulu efika ku-100 psi.
※ Ukufakwa kokuphela kwe-Luer-Lok okuhambisana nanoma yiziphi izinhlelo ezinkulu ze-flash emakethe.
※ Iyakwazi ukuhlangabezana nezidingo zokukhushulwa kwenqubo kusukela kwabancane kuya esikalini somshayeli.
※ Amakholomu e-flash apakishwe ngaphambili anika amandla ukugijima okusheshayo ukuze wonge isikhathi nezincibilikisi.
※ Umzimba wekholomu wepulasitiki olahlwayo unika amandla ukuphatha imfucuza okulula nokuphephile.
I-silica ehlanzekile kakhulu, 40–63 µm, 60 Å (Umkhiqizo OMUSHA)(indawo engaphezulu 500 m2/g, pH 6.5–7.5, umthamo wokulayisha 0.1–10%)
| Inombolo Yento | Usayizi Wekholomu | Usayizi Wesampula | Amayunithi/Ibhokisi | Izinga lokugeleza (mL/min) | Ubude beCartridge (mm) | I-Cartridge ID (mm) | Ubukhulu. Ingcindezi (psi/bar) |
| S-5101-5000 | 5 kg | 5 g - 500 g | 1 | 200–500 | 770 | 127.5 | 100/6.9 |
※ Iyahambisana nazo zonke izinhlelo ze-flash chromatography emakethe.
Ukuhlukana Okuhle nge-SepaFlash™ 5 kg
Isampula:I-Acetophenone ne-P-Methoxyacetophenone
Isigaba samaselula:80% hexane kanye 20% ethyl acetate
Isilinganiso sokugeleza:250 mL/min
Usayizi Wesampula:60 ml
Ubude begagasi:254 nm
Amapharamitha weChromatographic:
| Usayizi Wekholomu | tR | N | Rs | T |
| I-SepaFlash™ 5kg | 50 min | 617 | 6.91 | 1.00 |
※ Hlanza kufikela ku-1 kg wesampula ngokugijima okukodwa.
※ Ivalwe ngokukhethekile ngesu lobunikazi.
※ Ukusebenza okuthembekile, okungaguquki kusuka kuhlelo lokupakisha lobunikazi
※ Umzimba we-cartridge oqinisiwe onengcindezi yokusebenza ephezulu efika ku-100 psi (6.9bar)
※ Ama-adaptha ahlukahlukene amashubhu e-OD ahlukene ayenza ihambisane nanoma yiziphi izinhlelo ezinkulu ze-flash emakethe
※ Iyakwazi ukuhlangabezana nezidingo zokukhushulwa kwenqubo kusukela kwabancane kuya esikalini somshayeli
※ Amakholomu e-flash apakishwe ngaphambili anika amandla ukugijima okusheshayo ukuze wonge isikhathi nezincibilikisi
※ Umzimba wekholomu yepulasitiki elahlayo yenza kube lula futhi kuphephile ukuphatha imfucuza
I-silica ehlanzekile kakhulu, 40–63 µm, 60 Å (Umkhiqizo OMUSHA)(indawo engaphezulu 500 m2/g, pH 6.5–7.5, umthamo wokulayisha 0.1–10%)
| Inombolo Yento | Usayizi Wekholomu | Usayizi Wesampula | Amayunithi/Ibhokisi | Izinga lokugeleza (mL/min) | Ubude beCartridge (mm) | I-Cartridge ID (mm) | Ubukhulu. Ingcindezi (psi/bar) |
| I-S-5101-010K | 10 kg | 10 g - 1 kg | 1 | 300-1000 | 850 | 172.5 | 100/6.9 |
※ Iyahambisana nazo zonke izinhlelo ze-flash chromatography emakethe.
Ukuhlukaniswa Okuhle nge-SepaFlash™ 10 kg
Isampula:I-Acetophenone ne-P-Methoxyacetophenone
Isigaba samaselula:80% hexane kanye 20% ethyl acetate
Isilinganiso sokugeleza:400 mL/min
Usayizi Wesampula:100 ml
Ubude begagasi:254 nm
Amapharamitha weChromatographic:
| Usayizi Wekholomu | tR | N | Rs | T |
| I-SepaFlash™ 10kg | 65 imiz | 446 | 5.97 | 1.22 |
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