I-Sepaflash ™ Uchungechunge Olujwayelekile
Amakholomu we-Standard Series Flash agcwele i-Ultrapure Silica Gel usebenzisa inqubo yokupakisha eyomile eyomile.
※ I-Ultrapure Silica ifaka ukusatshalaliswa kosayizi oqinile, izinga eliphansi lenhlawulo kanye nokuqukethwe okuphansi kwensimbi, okuqukethwe okungathathi hlangothi, okuqukethwe okulawulwa kwamanzi kanye nendawo ephezulu yokuhlola
Indlela eyingqayizivele, ephathelene nokupakisha eyomile iqinisekisa ukulungiswa okuphezulu kanye nokuvela kabusha kokuhlanzwa kwansuku zonke.
※ ingcindezi ethuthukisiwe ilinganiselwe ku-300 PSI
| Inombolo yento | Usayizi wekholomu | Usayizi wesampula (g) | I-Flow Rate (ML / Min) | Ubude be-cartridge (cm) | I-id ye-cartridge (mm) | UMax. Ingcindezi (PSI / Bar) | Inani / Ibhokisi | |
| -Ncinyane | -Ningi | |||||||
| S-5101-0004 | 4 g | 4 mg-0.4 g | 15-40 | 105.8 | 12.4 | 300 / 20.7 | 36 | I-120 |
| S-5101-0012 | 12 g | 12 mg-1.2 g | 30-60 | 124.5 | 21.2 | 300 / 20.7 | 24 | I-108 |
| S-5101-0025 | 25 g | 25 mg-2.5 g | 30-60 | 172.7 | 21.3 | 300 / 20.7 | 20 | 80 |
| S-5101-0040 | 40 g | 40 mg-4.0 g | 40-70 | 176 | 26.7 | 300 / 20.7 | 15 | 60 |
| S-5101-0080 | 80 g | 80 mg-8.0 g | 50-100 | 248.5 | 30.9 | 200 / 13.8 | 10 | 20 |
| S-5101-0120 | 120 g | I-120 mg-12 g | 60-150 | 261.5 | 37.2 | 200 / 13.8 | 8 | 16 |
| S-5101-0220 | 220 g | 220 mg-22 g | 80-220 | 215.9 | 59.4 | 150 / 10.3 | 4 | 8 |
| S-5101-0330 | 330 g | 330 mg-33 g | 80-220 | 280.3 | 59.8 | 150 / 10.3 | 3 | 6 |
| S-5101-0800 | 800 g | I-800 mg-80 g | 100-300 | 382.9 | 78.2 | I-100 / 6.9 | 3 | / |
| S-5101-1600 | 1600 g | 1.6 g-160 g | 200-500 | 432.4 | 103.8 | I-100 / 6.9 | 2 | / |
| S-5101-3000 | 3000 g | 3.0 g-300 g | 200-500 | 509.5 | 127.5 | I-100 / 6.9 | 1 | / |
※ iyahambisana nazo zonke izinhlelo ze-chromatography ye-flash emakethe.
| Inombolo yento | Usayizi wekholomu | Usayizi wesampula(g) | Izinga Lokugeleza(ml / min) | Ubude be-cartridge(cm) | I-id ye-cartridge(MM) | UMax. Ukucindezela(PSI / Bar) | Inani / Ibhokisi | |
| -Ncinyane | -Ningi | |||||||
| S-8601-0004-n | 8 g | 8 mg-0.32 g | 10-30 | 105.8 | 12.4 | 300 / 20.7 | 36 | I-120 |
| S-8601-0012-n | 24 g | 24 mg-1.0 g | 15-45 | 124.5 | 21.2 | 300 / 20.7 | 24 | I-108 |
| S-8601-0025-n | 50 g | 50 mg-2.0 g | 15-45 | 172.7 | 21.3 | 300 / 20.7 | 20 | 80 |
| S-8601-0040-n | 80 g | 80 mg-3.2 g | 20-50 | 176 | 26.7 | 300 / 20.7 | 15 | 60 |
| S-8601-0080-n | 160 g | I-160 mg-6.4 g | 30-70 | 248.5 | 30.9 | 200 / 13.8 | 10 | 20 |
| S-8601-0120-N | 240 g | 240 mg-9.6 g | 40-80 | 261.5 | 37.2 | 200 / 13.8 | 8 | 16 |
| S-8601-0220-N | 440 g | 440 mg-17.6 g | 50-120 | 215.9 | 59.4 | 150 / 10.3 | 4 | 8 |
| S-8601-0330-n | 660 g | I-660 mg-26.4 g | 50-120 | 280.3 | 59.8 | 150 / 10.3 | 3 | 6 |
| S-8601-0800-n | 1600 g | 1.6 g-64 g | 100-200 | 382.9 | 78.2 | I-100 / 6.9 | 3 | / |
| S-8601-1600-n | 3200 g | 3.2 g-128 g | 150-300 | 432.4 | 103.8 | I-100 / 6.9 | 2 | / |
| S-8601-3000-n | I-6000 g | 6.0 g-240 g | 150-300 | 509.5 | 127.5 | I-100 / 6.9 | 1 | / |
※ iyahambisana nazo zonke izinhlelo ze-chromatography ye-flash emakethe.
Amakholomu weSepaflash ™ Flash anikela ngokusebenza kahle ngemikhiqizo yokuncintisana ngenxa yekhwalithi ephezulu ye-Silica Gel kanye nendlela yokupakisha entsha.
Lokhu okusebenzayo okusebenzayo kunesakhiwo sezinhlayiyana esingajwayelekile okunemiphetho ebushelelezi, ukusatshalaliswa kosayizi omncane kakhulu kanye nezinga eliphansi lenhlawulo enikelwe yiSantai, okuzokwenza isikhathi sakho nemali. Ijeli ye-silica engajwayelekile inezinhlobo ezimbili zokucaciswa, 40-63 μm no-25-40 μm. Ikakhulu, uSantai uphinde athuthukise inqubo eqinile yokupakisha eyomile yama-silica angajwayelekile angama-25- 40 μm, kanye nama-cartidge angaphambi kwangaphambi kwama-25- 40
Isithombe se-40-63 μm silica gel
USantai Gel weSilica futhi unikeza lezi zinzuzo ngaphezulu kwemikhiqizo yokuncintisana:
I-Houtral Ph:I-PH ye-Silica Gel ye-Silica ye-Santai igcinwa phakathi kuka-6.5-7.5. I-ph engathathi hlangothi iyadingeka ukuhlukanisa amakhompiyutha abucayi be-PH.
Okuqukethwe emanzini okuzinzile:Okuqukethwe kwamanzi kwe-silica gel kungathinta ukhetho lwe-silica. I-Silica Gel kaSantai engajwayelekile inokuqukethwe kwamanzi okulawulwayo kwe-4% kuya ku-6%.
Indawo ephezulu yendawo:Indawo ephezulu engaphezulu (500 m2/ g ngosayizi ka-60 Å) unikeza amandla amakhulu wokuhlukanisa.
Ukusatshalaliswa kosayizi oqinile wezinhlayiya kanye ne-batch-to-batch-to-batch yokusatshalaliswa okuphezulu Ukuvela okuphezulu kwe-batch-to-batch kokusatshalaliswa kosayizi wezinhlayiyana okuyisisekelo kuqinisekisa ukusebenza okuhle kakhulu kokuhlukanisa. Imininingwane engaphezulu sicela ubheke isithombe se-sem kanye nokusatshalaliswa kosayizi wezinhlayiyana zamabhendi amabili.
Ukusatshalaliswa kosayizi wezinhlayiyana kwamabhathi amabili ama-40-63 μm ne-25- 40 μM silica gel
Amakholomu weSepaflash ™ manje ayatholakala ngosayizi we-5 kg.
okungahlanza amagremu afinyelela kuma-500 wesampula ngokugijima okukodwa.
I-Spin-Welded futhi ingama ingcindezi kuze kube yi-100 PSI (6.9 Bar).
※ ukusebenza okuthembekile, okungaguquki kusuka kwinqubo yokupakisha yokuphathelene.
※ umzimba we-cartridgedced eqiniswe ngokucindezela okusebenzayo kuze kube yi-100 PSI.
※ ukufakwa kokuphela kokuphela kwe-Luer-Lok kuyahambisana nanoma yiziphi izinhlelo ezinkulu ze-Flash emakethe.
※ ukwazi ukufeza izidingo zenqubo yokulinganisa kusuka ezikalini ezincane kuya kwesilinganiso somshayeli.
※ Amakholomu we-Flash agcwele ngaphambili anika amandla okuhlanza ngokushesha ukugijima ukonga isikhathi nama-solvents.
※ ukulahlwa komzimba wekholamu epulasitiki Nika amandla ukuphathwa kwemfucuza okulula nokuphephile.
I-Silica Engajwayelekile ye-Ultra-emsulwa, 40-63 μm, 60 Å (Umkhiqizo omusha)(indawo ephezulu engu-500 m2/ g, ph 6.5-7.5, Kulayishwa umthamo 0.1-10%)
| Inombolo yento | Usayizi wekholomu | Usayizi wesampula | Amayunithi / ibhokisi | I-Flow Rate (ML / Min) | Ubude be-cartridge (mm) | I-id ye-cartridge (mm) | UMax. Ingcindezi (PSI / Bar) |
| S-5101-5000 | 5 kg | I-5 g-500 g | 1 | 200-500 | I-770 | 127.5 | I-100 / 6.9 |
※ iyahambisana nazo zonke izinhlelo ze-chromatography ye-flash emakethe.
Ukuhlukaniswa okuhle nge-sepaflash ™ 5 kg
Isampula:I-Acetophenone ne-P-Methoxyacetonenone
Isigaba seselula:80% uHexane no-20% ethyl acetate
I-Flow Rate:250 ml / min
Isampula usayizi:60 ml
Ubude be-Wave:254 nm
Amapharamitha we-Chromatographic:
| Usayizi wekholomu | tR | N | Rs | T |
| I-Sepaflash ™ 5kg | I-50min | I-617 | I-6.91 | 1.00 |
※ hlanza kuze kufike ku-1 kg wesampula ngokugijima okukodwa.
※ ivalwe ngokuqondile ngenqubo yokuphathelene.
※ ukusebenza okuthembekile, okuguqukayo kusuka kwinqubo yokupakisha yokuphathelene
※ umzimba we-cartridgedced cartridge ngengcindezi yokusebenza ephezulu kuze kube yi-100 PSI (6.9Bar)
※ adaptha ahlukahlukene amashubhu ahlukene we-od awenza maqondana nanoma yiluphi uhlelo olukhulu lwe-flash emakethe
※ ukwazi ukufeza izidingo zenqubo yokulinganisa kusuka esikalini esincane kuya ku-Pilot-Scale
※ Amakholomu we-Flash Pread Pred afakwe amandla okuhlanza ngokushesha ukulondolozwa isikhathi nama-solvents
※ ukulahlwa komzimba wekholamu epulasitiki Nika amandla ukuphathwa kwemfucuza okulula nokuphephile
I-Silica Engajwayelekile ye-Ultra-emsulwa, 40-63 μm, 60 Å (Umkhiqizo omusha)(indawo ephezulu engu-500 m2/ g, ph 6.5-7.5, Kulayishwa umthamo 0.1-10%)
| Inombolo yento | Usayizi wekholomu | Usayizi wesampula | Amayunithi / ibhokisi | I-Flow Rate (ML / Min) | Ubude be-cartridge (mm) | I-id ye-cartridge (mm) | UMax. Ingcindezi (PSI / Bar) |
| S-5101-010K | 10 kg | I-10 g-1 kg | 1 | I-300-1000 | I-850 | 172.5 | I-100 / 6.9 |
※ iyahambisana nazo zonke izinhlelo ze-chromatography ye-flash emakethe.
Ukuhlukaniswa okuhle ngeSepaflash ™ 10 kg
Isampula:I-Acetophenone ne-P-Methoxyacetonenone
Isigaba seselula:80% uHexane no-20% ethyl acetate
I-Flow Rate:I-400 ml / min
Isampula usayizi:I-100 ml
Ubude be-Wave:254 nm
Amapharamitha we-Chromatographic:
| Usayizi wekholomu | tR | N | Rs | T |
| I-Sepaflash ™ 10kg | I-65min | 446 | I-5.97 | 1.22 |
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Ikhathalogi ye-Sepaflash Colum en
- Ukusetshenziswa kwe-AN-008 Ukusetshenziswa kwe-Santai Sepaflash ™ Ikholomu yokuhlanzwa komkhiqizo wemvelo wemvelo ekwandulweni kwama-gram amaningi
- Imikhiqizo emikhulu yokuhlanza imikhiqizo emikhulu yamakhulu amagremu wamasampula
- I-AN007_Ukusetshenziswa komshini we-Sepabean ™ emkhakheni wezinto zokwenziwa kwe-Organic Optoelectronic
- I-AN011_TTING Insight emshinini we-Sepabean ™ nonjiniyela: umtshina wokuhlakazeka wokukhanya okuguqukayo
- I-A021_Ukusebenza kwekholomu ifaka ekuhlanzeni kwezinto eziphilayo ze-Orpolectronic
- I-AN024_Ukusetshenziswa kwe-orthogonal chromatography yokuhlanzwa kwemiphakathi yokwenziwa yezemithi
