ISepaFlash™ Uthotho oluMgangatho
Iikholamu ze-Standard Series flash zifakwe ngoomatshini ngejeli ye-silica ye-UltraPure usebenzisa ubuchule bokupakisha okomileyo.
※ I-silica ye-UltraPure ibonakalisa ukusabalalisa ubungakanani besuntswana, inqanaba eliphantsi lezohlwayo kunye nomxholo ophantsi wesinyithi, i-pH engathathi hlangothi, umxholo wamanzi olawulwayo kunye nommandla ophezulu, ukubonelela izazinzulu iziphumo zovavanyo ezifunwayo.
※ Ubuchule bokupakisha okomileyo obukhethekileyo buqinisekisa isisombululo esiphezulu kunye nokuphindaphinda ukucocwa kwemihla ngemihla.
※ Uxinzelelo oluphuculweyo lulinganiswe ukuya kuthi ga kwi-300 psi
| Inombolo yento | Ubungakanani beKholam | Ubungakanani beSampuli(g) | Inqanaba lokuHamba(mL/min) | Ubude beCartridge (cm) | ICartridge ID (mm) | Max. Uxinzelelo (psi/bar) | Ubuninzi / Ibhokisi | |
| Incinci | Enkulu | |||||||
| S-5101-0004 | 4 g | 4 mg–0.4 g | 15–40 | 105.8 | 12.4 | 300/20.7 | 36 | 120 |
| S-5101-0012 | 12 g | 12 mg–1.2 g | 30–60 | 124.5 | 21.2 | 300/20.7 | 24 | 108 |
| S-5101-0025 | 25 g | 25 mg–2.5 g | 30–60 | 172.7 | 21.3 | 300/20.7 | 20 | 80 |
| S-5101-0040 | 40 g | 40 mg–4.0 g | 40–70 | 176 | 26.7 | 300/20.7 | 15 | 60 |
| S-5101-0080 | 80 g | 80 mg–8.0 g | 50–100 | 248.5 | 30.9 | 200/13.8 | 10 | 20 |
| S-5101-0120 | 120 g | 120 mg–12 g | 60–150 | 261.5 | 37.2 | 200/13.8 | 8 | 16 |
| S-5101-0220 | 220 g | 220 mg–22 g | 80–220 | 215.9 | 59.4 | 150/10.3 | 4 | 8 |
| S-5101-0330 | 330 g | 330 mg–33 g | 80–220 | 280.3 | 59.8 | 150/10.3 | 3 | 6 |
| S-5101-0800 | 800 g | 800 mg–80 g | 100–300 | 382.9 | 78.2 | 100/6.9 | 3 | / |
| S-5101-1600 | 1600 g | 1.6 g–160 g | 200–500 | 432.4 | 103.8 | 100/6.9 | 2 | / |
| S-5101-3000 | 3000 g | 3.0 g–300 g | 200–500 | 509.5 | 127.5 | 100/6.9 | 1 | / |
※ Iyahambelana nazo zonke iinkqubo zekhromatografi kwimarike.
| Inombolo yento | Ubungakanani beKholam | Ubungakanani beSampuli(g) | Umgangatho wohambo(mL/min) | Ubude beCartridge(i-cm) | ICartridge ID(mm) | Max. Uxinzelelo(psi/bar) | Ubuninzi / Ibhokisi | |
| Incinci | Enkulu | |||||||
| S-8601-0004-N | 8 g | 8 mg–0.32 g | 10–30 | 105.8 | 12.4 | 300/20.7 | 36 | 120 |
| S-8601-0012-N | 24 g | 24 mg–1.0 g | 15–45 | 124.5 | 21.2 | 300/20.7 | 24 | 108 |
| S-8601-0025-N | 50 g | 50 mg–2.0 g | 15–45 | 172.7 | 21.3 | 300/20.7 | 20 | 80 |
| S-8601-0040-N | 80 g | 80 mg–3.2 g | 20–50 | 176 | 26.7 | 300/20.7 | 15 | 60 |
| S-8601-0080-N | 160 g | 160 mg–6.4 g | 30–70 | 248.5 | 30.9 | 200/13.8 | 10 | 20 |
| S-8601-0120-N | 240 g | 240 mg–9.6 g | 40–80 | 261.5 | 37.2 | 200/13.8 | 8 | 16 |
| S-8601-0220-N | 440 g | 440 mg–17.6 g | 50–120 | 215.9 | 59.4 | 150/10.3 | 4 | 8 |
| S-8601-0330-N | 660 g | 660 mg–26.4 g | 50–120 | 280.3 | 59.8 | 150/10.3 | 3 | 6 |
| S-8601-0800-N | 1600 g | 1.6 g–64 g | 100–200 | 382.9 | 78.2 | 100/6.9 | 3 | / |
| S-8601-1600-N | 3200 g | 3.2 g–128 g | 150–300 | 432.4 | 103.8 | 100/6.9 | 2 | / |
| S-8601-3000-N | 6000 g | 6.0 g–240 g | 150–300 | 509.5 | 127.5 | 100/6.9 | 1 | / |
※ Iyahambelana nazo zonke iinkqubo zekhromatografi kwimarike.
Iikholamu zombane zeSepaFlash™ zibonelela ngokusebenza okumangalisayo kwiimveliso ezikhuphisanayo ngenxa yomgangatho ophezulu wejeli yesilica kunye nobuchule bokupakisha obutsha.
Esi sixhobo siphezulu sinomfanekiso ongaqhelekanga wamasuntswana kunye nemiphetho egudileyo, ukusabalalisa ubungakanani beqhekeza elincinci kakhulu kunye nezinga eliphantsi lezohlwayo ezinikezelwa nguSantai, eziza kwandisa amandla akho okwahlula kwaye ugcine ixesha lakho kunye nemali. Ijeli ye-silica engaqhelekanga ineendidi ezimbini zengcaciso, 40-63 µm kunye ne-25-40 µm. Ngokukodwa, uSantai uphuhlisa ngakumbi indlela yokupakisha eyomileyo ezinzileyo ye-silica eyi-25-40 µm, kunye ne-silica cartridges epakishwe ngaphambili eyi-25-40 µm iya kubonisa isakhono esingaqhelekanga ekujonganeni nokwahlula.
Umfanekiso we-SEM we-40-63 μm i-silica gel
Ijeli ye-silica yeSantai ikwabonelela ngezi nzuzo ngaphezu kweemveliso zokhuphisana nabo:
I-pH ephakathi:I-pH yejeli ye-silica ye-Santai igcinwa phakathi kwe-6.5−7.5. I-pH engathathi hlangothi iyafuneka ukwahlula iikhompawundi ezibuthathaka ze-pH.
Isiqulatho samanzi esizinzileyo:Umxholo wamanzi we-silica gel unokuchaphazela ukukhethwa kwe-silica. Ijeli ye-silica ye-Santai engaqhelekanga inomthamo wamanzi olawulwayo we-4% ukuya kwi-6%.
Umgangatho ophezulu:Indawo engaphezulu (500 m2/g ye-60 Å ubukhulu bepore) inika amandla amakhulu okwahlula.
Ukusabalalisa ubungakanani be-particle kunye ne-batch-to-batch reproducibility: Ukusabalalisa ubungakanani be-particle encinci kuya kunika ukupakishwa kwe-homogenous ukuqokelela amaqhezu agxininisiweyo kunye nokunciphisa ukusetyenziswa kwe-solvent, okuya kunciphisa iindleko ngokubanzi. Ukuveliswa kwakhona kwebhetshi ukuya kwibhetshi yobungakanani bobungakanani bamasuntswana kuqinisekisa ngokusisiseko ukusebenza kakuhle kokwahlula. Iinkcukacha ezingakumbi nceda ubone umfanekiso we-SEM kunye nokusabalalisa ubungakanani be-particle yeebhetshi ezimbini.
Ukuhanjiswa kobungakanani benxalenye yeebhetshi ezimbini ze-40-63 μm kunye ne-25-40 μm ijeli yesilika
Iikholamu zeSepaFlash™ ngoku zifumaneka ngesayizi ye-5 kg.
enokuhlambulula ukuya kuthi ga kwi-500 grams yesampuli ngexesha elinye.
I-spin-welded kwaye inokumelana noxinzelelo ukuya kwi-100 psi (i-6.9 bar).
※ Ukuthembeka, ukusebenza okungaguqukiyo ukusuka kubuchule bokupakisha bobunini.
※ Umzimba wekhatriji owomeleziweyo kunye noxinzelelo oluphezulu lokusebenza ukuya kuthi ga kwi-100 psi.
※ Luer-Lok isiphelo fittings iyahambelana naziphi na iinkqubo flash ezinkulu kwimarike.
※ Ukwazi ukuhlangabezana neemfuno zenkqubo yokunyuswa komgangatho ukusuka kwinqanaba elincinci ukuya kwinqanaba lokulingwa.
※ Iikholamu zombane ezipakishwe kwangaphambili zivumela ukucocwa ngokukhawuleza ukonga ixesha kunye nezinyibilikisi.
※ Umzimba wekholamu yeplastiki elahlayo yenza kube lula kwaye kukhuseleke ukuphatha inkunkuma.
I-silica ecocekileyo kakhulu, i-40–63 µm, 60 Å (iMveliso ENTSHA)(ummandla ongaphezulu kwama-500 m2/g, pH 6.5-7.5, umthamo wokulayisha 0.1-10%)
| Inombolo yento | Ubungakanani beKholam | Ubungakanani beSampuli | Iiyunithi/Ibhokisi | Inqanaba lokuHamba (mL/min) | Ubude beCartridge (mm) | ICartridge ID (mm) | Max. Uxinzelelo (psi/bar) |
| S-5101-5000 | 5kg | 5 g–500 g | 1 | 200–500 | 770 | 127.5 | 100/6.9 |
※ Iyahambelana nazo zonke iinkqubo zekhromatografi kwimarike.
Ukwahlula okulungileyo kunye ne-SepaFlash™ 5 kg
Isampulu:I-Acetophenone kunye ne-P-Methoxyacetophenone
Isigaba esiphathwayo:I-80% ye-hexane kunye ne-20% ye-ethyl acetate
Umgangatho wohambo:250 mL / min
Isampulu yobungakanani:60 ml
Ubude beMaza:254 nm
Iiparamitha zeChromatographic:
| Ubungakanani beKholam | tR | N | Rs | T |
| SepaFlash™ 5kg | 50min | 617 | 6.91 | 1.00 |
※ Hlanza ukuya kuthi ga kwi-1 kg yesampuli ngokubaleka okukodwa.
※ Itywinwe ngokukodwa ngobuchule bobunini.
※ Ukuthembeka, ukusebenza okungaguqukiyo ukusuka kubuchule bokupakisha bobunini
※ Umzimba wekhatriji owomeleziweyo kunye noxinzelelo oluphezulu lokusebenza ukuya kuthi ga kwi-100 psi (6.9bar)
※ Iiadaptha ezahlukeneyo zeetyhubhu zeOD ezahlukeneyo zenza ukuba ihambelane nazo naziphi na iinkqubo ezinkulu zombane kwimarike
※ Ukwazi ukuhlangabezana neemfuno zenkqubo yokunyuswa komgangatho ukusuka kwinqanaba elincinci ukuya kwinqanaba lokulingwa
※ Iikholamu zombane ezipakishwe kwangaphambili zivumela ukucocwa ngokukhawuleza ukonga ixesha kunye nezinyibilikisi
※ Umzimba wekholamu yeplastiki elahlayo yenza kube lula kwaye kukhuseleke ukuphatha inkunkuma
I-silica ecocekileyo kakhulu, i-40–63 µm, 60 Å (iMveliso ENTSHA)(ummandla ongaphezulu kwama-500 m2/g, pH 6.5-7.5, umthamo wokulayisha 0.1-10%)
| Inombolo yento | Ubungakanani beKholam | Ubungakanani beSampuli | Iiyunithi/Ibhokisi | Inqanaba lokuHamba (mL/min) | Ubude beCartridge (mm) | ICartridge ID (mm) | Max. Uxinzelelo (psi/bar) |
| S-5101-010K | 10 kg | 10 g-1 kg | 1 | 300-1000 | 850 | 172.5 | 100/6.9 |
※ Iyahambelana nazo zonke iinkqubo zekhromatografi kwimarike.
Ukwahlula okulungileyo ngeSepaFlash™ 10 kg
Isampulu:I-Acetophenone kunye ne-P-Methoxyacetophenone
Isigaba esiphathwayo:I-80% ye-hexane kunye ne-20% ye-ethyl acetate
Umgangatho wohambo:400 mL / min
Isampulu yobungakanani:100 ml
Ubude beMaza:254 nm
Iiparamitha zeChromatographic:
| Ubungakanani beKholam | tR | N | Rs | T |
| I-SepaFlash™ 10kg | 65min | 446 | 5.97 | 1.22 |
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AN-SS-008 Ukusetyenziswa kwekholamu yeSantai SepaFlash™ yokuCoca iSandulela seMveliso yeNdalo kwisikali se-Multi-gram - AN005_SepaFlash™ iiMveliso ezinkulu zokuCoca kumakhulu eegram zeSampuli
- AN007_Ukusetyenziswa koMatshini we-SepaBean™ kwiNdawo ye-Organic Optoelectronic Materials
- AN011_Fumana ukuqonda kuMatshini weSepaBean™ oneNjineli: Isitshici sokuSasaza isiKhanya esiEvaporative
- AN021_Ukusetyenziswa kokupakishwa kweKholam ekuCocisweni kweMathiriyeli ye-Optoelectronic ye-Organic
- AN024_Ukusetyenziswa kweChromatography ye-Orthogonal yokuSungula i-Synthetic Pharmaceutical Intermediates
- SepaFlash ikholamu yeKhathalogu EN
