I-FAQS

I-Santaii ye-Santai Solvent TIT kunye nezixhobo

Hayi, i-silica esikhundleni esingena-suble singena kwisolokhwe esiqhelekileyo seSolntvent.

Ukucocwa ngokugqibeleleyo kunye ne-C18 Iikholamu zeF18, nceda ulandele la manyathelo:
① Funkse ikholamu nge-100% ye-SOFTE (i-organic) ye-10 - 20 cvs (ivolumu yekholamu), i-metanol okanye i-acetolile.
② Shukuma kwikholamu nge-50% yomelele + i-50% i-50% i-artives (ukuba iyafuneka, zibandakanye enye) kwenye enye 3 - 5 cvs.
③ Funkse ikholamu kunye neemeko zokuqala ze-3 - 5 cvs.

Ubungakanani bekholamu phakathi kwe-4G kunye ne-330g, isinxibelelanisi se-Lueer esisiseko esisetyenziswa kwezi kholan zeFlash. Ubungakanani bekholamu engama-800g, i-1600g kunye ne-3000g, i-Adapter Adract, iAdaptha eyongezelelweyo kufuneka isetyenziselwe ukonga iikholamu ezinkulu zeflash kwiNkqubo ye-Flash ye-flash chromatographys. Nceda ujonge kwi-Adapter ye-SADAI ye-adapter ye-ADYAI ye-800G, i-1600g, iikholamu ze-3KG ze-3KG i-3K

Kwindawo eqhelekileyo yenqanaba eliqhelekileyo, kuyacetyiswa ukuba isebenzise iSigaba seSoftware apho umyinge weMetanol akadluli kwi-25%.

Ngokubanzi, kuyacetyiswa ukuba basebenzise iSigaba seSoftway apho umyinge wemifanekiso engu-polar ayidluli kwi-5%. Izicoci ze-polar zibandakanya i-DMSO, i-DMF, i-thf, iti njl.njl.

Isampulu yesampulu yinto eluncedo yokulayisha isampulu ukuze ihlanjululwe kwikholamu, ngakumbi iisampulu zomhlaba ophantsi. Kule meko, i-Ilok Flash Cartridge yeyona nto ifanelekileyo.
Ngokubanzi, isampulu ichithwe kwi-solvent efanelekileyo kwaye ikhutshiwe kwi-adsorbant eqinileyo enokufana ne-Flash Plasms, kubandakanya umhlaba we-diatomaceous okanye izilwanyana okanye ezinye izinto. Emva kokususwa / ukuvela kweSolntrent School, i-adsorbent ibekwe ngaphezulu kwekholam egcwaliswe ngokuyinxalenye okanye kwi-carridge engenanto. Ngolwazi oluthe kratya ngakumbi, nceda ujonge kwi-Ilk-sl cartridge yesikhokelo soMsebenzisi ngeenkcukacha ezithe kratya.

Ivolumu yekholamu imalunga ne-volumu efileyo (vm) xa ungayihoyi ivolumu eyongezelelweyo kwiityhubhu ezixhuma ikholamu kunye ne-ijector.

Ixesha elifileyo (tm) lixesha elifunekayo lokufumana icandelo lezinto ezingabanjwanga.

Umthamo ofileyo (VM) ngumthamo wesigaba sefowuni efunekayo ukuze ube licandelo lezinto ezingabanjwanga. Ivolumu efileyo inokubalwa ngala manyala alandelayo: VM = F0 * I-TM.

Phakathi kwale nyala ingentla, i-F0 ngumgangatho wokuhamba kwesigaba sefowuni.

Hayi, i-silica esikhundleni esingena-suble singena kwisolokhwe esiqhelekileyo seSolntvent.

Ikholamu ye-Silica Flash Ikholamu iyalahleka kwaye isetyenziselwe okungatshatanga, kodwa ngokuphatha ngendlela efanelekileyo, iikhareji ze-silica carridge zingaphinde ziphinde ziphinde zibuncame ukusebenza.
Ukuze iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde iphinde isebenze, ikholamu ye-Silica Flash kufuneka yomiswe nje ngumoya oxinzelelweyo okanye ityiwe kunye kwaye igcinwe kwi-Iyopropanol.

Ukugcina ngokufanelekileyo kuya kuvumela iikholamu ze-C18 ze-flash ukuze ziphinde zisetyenziswe:
• Ungaze uvumele ikholamu ukuba yome emva kokusebenzisa.
• Susa zonke iindlela ze-organic ngokutyibilika kwikholamu nge-80% Methanol okanye i-acetotile emanzini ama-3 - 5 cvs.
• Gcina ikholamu kwi-solven ekhankanywe apha ngasentla enezixhobo zokuphela.

Kwiikholamu ezinkulu ezikhulu ngaphezulu kwe-220g, isiphumo se-thermal sicacile kwinkqubo yokuthengisa kwangaphambili. Kucetyiswa ukuseta ireyithi yokuhamba kwi-50-60% yeqondo lokuhamba elicetyiswayo kwiNkqubo yeNkqubo yokuThintela kwangaphambili ukunqanda isiphumo se-therifal.

Isiphumo se-thermal ye-solventi exutyweyo icace veta ngakumbi kune-solvent enye. Thatha inkqubo ye-SOLCLOHXAYE / YENYL Acetate njengomzekelo, kucetyiswa ukuba usebenzise i-100% ye-cyclohexane ngenkqubo yangaphambi kokulingana. Xa ulungelelwaniso lwangaphambi kokuba ulungelwe, ulindelo lokwahlula-hlulwa lunokwenziwa ngokwenkqubo yokuyiswa kwesekiweyo.